Scheme of Instruction and Evaluation for M. Pharmacy




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Osmania University


Syllabus for M. Pharmacy

(Pharmaceutical Chemistry)

(w.e.f. academic year 2009-10)


Faculty of Technology,

Hyderabad


Scheme of Instruction and Evaluation for M. Pharmacy

(Pharmaceutical Chemistry)

I – Semester



Subject Code

Subject / Paper

Theory / Practical

Instruction Hours per week

Evaluation

Duration of External Examination
















Theory

Practical

Internal

External




M PCH.T.1.101

Pharmaceutical Analytical Techniques

Theory

4



30

70

3

M PCH.T.1.102

Advanced Pharmaceutical Organic Chemistry – I

Theory

4



30

70

3

M PCH.T.1.103

Advanced Medicinal Chemistry – I

Theory

4



30

70

3

M PCH.T.1.104

Advanced Chemistry of Natural Products

Theory

4



30

70

3

M PCH.P.1.105

Pharmaceutical Analytical Techniques

Practical



6

30

70

6

M PCH.P.1.106

Advanced Chemistry of Natural Products

Practical



6

30

70

6

M PCH.T.1.107

Entrepreneurship Management (SAIL)

Tutorials

2



A/B/C/D





M PCH.1.108

Seminar





8

50
















18

20

230

420






Scheme of Instruction and Evaluation for M. Pharmacy

(Pharmaceutical Chemistry)

II– Semester



Subject Code

Subject / Paper

Theory / Practical

Instruction Hours per week

Evaluation

Duration of External Examination
















Theory

Practical

Internal

External




M PCH.T.1.201

Intellectual Property Rights & Regulatory Affairs

Theory

4



30

70

3

M PCH.T.1.202

Advanced Pharmaceutical Organic Chemistry – II

Theory

4



30

70

3

M PCH.T.1.203

Advanced Medicinal Chemistry – II

Theory

4



30

70

3

M PCH.T.1.204

Drug Screening Methods & Biostatistics

Theory

4



30

70

3

M PCH.P.1.205

Advanced Pharmaceutical Organic Chemistry – II

Practical



6

30

70

6

M PCH.P.1.206

Advanced Medicinal Chemistry – II

Practical



6

30

70

6

M PCH.T.1.207

Scientific and Technical Writing (SAIL)

Tutorials

2



A/B/C/D





M PCH.T.1.208

Seminars





8

50














18

20

230

420






SAIL: Self assess Instrumentation Learning


Scheme of Instruction and Evaluation for M. Pharmacy

(Pharmaceutical Chemistry)


Semester III and IV

DISSERTATION – Original research work carried out by the candidate under the guidance of regular teaching faculty/visiting faculty of the department should be submitted in a bound form.

Evaluation of the dissertation shall be done by external and internal examiners appointed by the university.

Dissertation viva-voce Grade A/B/C/D/F

Dissertation report Grade A/B/C/D/F

A: Excellent B. Very good C. Good D: Fair F. Fail


PHARMACEUTICAL ANALYTICAL TECHNIQUES

M PCH.T.1.101 Period/Week: 4

Sessional: 30 Duration of Exam: 3 hrs

Examination: 70 Nature of Exam: Theory

UNIT – I

a) UV-Visible Spectroscopy: Basic principles, interaction of electromagnetic radiation with matter and its effects (electronic transitions). Concept of chromophore and auxochrome, effect of conjugation, solvent and pH. Instrumentation (components and their significance). Absorption spectra of organic compounds and complexes illustrating the phenomenon and its utilization in qualitative and quantitative studies of drugs including multicomponent analysis. Woodward-Fieser rules for caculating absortion maximum for unsaturated hydrocarbons. Difference and derivative spectra.

b) Infra-Red Spectroscopy: Interaction of infrared radiation with organic molecules and it’s effects on bonds. Instrumentation- Dispersive IR spectrophotometers and Fourier transform spectrophotometers. Sample handling for IR spectroscopy. Interpretation of IR spectra. Brief note on ATR. (Attenuated Total Reflectance).

UNIT – II

Nuclear Magnetic Resonance Spectroscopy: Fundamental principles of NMR, instrumentation (components and their significance). Chemical shifts concept, spin- spin coupling, spin-spin decoupling, shielding and deshielding, solvents. signal multiplicity phenomena in high resolution PMR. Interpretation of PMR spectra.

Brief introduction about Carbon-13 NMR and 2D NMR Spectroscopy.

UNIT – III

Mass Spectrometry: Basic principles and instrumentation (components and their significance). Ionization techniques, mass spectrum and its characteristics, molecular ion, metastable ions, fragment ions; fragmentation processes, fragmentation patterns and fragment characteristics in relation to parent structure and functional groups. Relative abundances of isotopes and their contribution to characteristic peaks.

UNIT – IV

Chromatographic Techniques: Classification of chromatographic methods based on mechanism of separation and their basic principles. Gas chromatography: Instrumentation, column efficiency parameters, derivatisation methods, applications in pharmaceutical analysis. Liquid chromatography: Comparison of GC and HPLC, instrumentation in HPLC, normal and reversed phase packing materials, column selection, mobile phase selection, efficiency parameters, applications in pharmaceutical analysis. Instrumentation and applications of HPTLC, ion exchange chromatography, gel permeation chromatography, chiral chromatography, flash chromatography, and supercritical fluid chromatography (SFC).

UNIT – V

a) Electrophoresis: Principles, instrumentation and applications of moving boundary electrophoresis, zone electrophoresis (ZE), isotachphoresis, isoelectric focusing (IEF), continous electrophoresis (preparative) and capillary electrophoresis. SDS gel electrophoresis and blotting techniques.

b) Radio immunoassay and ELISA: Principle, instrumentation, applications and limitations.



Recommended Books:

  1. 1. Skoog, DA, Holler, FJ, Crouch, SR. Principles of instrumental analysis. 6th ed., Baba Barkha Nath printers, Haryana, 2007.

  2. 2. Silverstein, RM, Webstar, FX. Spectrometric identification of organic compounds. 6th ed., John Wiley & Sons (Asia) Pvt. Ltd., Singapore, 2005.

  3. 3. William Kemp. Organic spectroscopy, 3rd ed., Palgrave, New York, 2006.

  4. 4. Jag Mohan, Organic spectroscopy: Principles and Applications, 2nd ed., Narosa publishing house Pvt Ltd., New Delhi, 2005.

  5. 5. Conners KA. A Text book of pharmaceutical analysis, 3rd ed., John Wiley & Sons, Singapore, 2004.

  6. 6. Willard HH, Merritt LL, Dean JA, Settle FA. Instrumental methods of analysis, 7th ed., CBS Publishers & Distributors, New Delhi, 1986.

  7. 7. Pavia DL, Lampman GM, Kriz GS, Vyvyan JA. Introduction to spectroscopy. 4th ed., Brookescole publishers, California, 2008.

  8. 8. Sharma BK. Instrumental methods of chemical analysis, 25th Ed., Goel Publishing house, Meerut, 2006.

  9. 9. Beckett, AH, Stenlake, JB. Practical pharmaceutical chemistry, Part I & II, 4th ed., CBS Publishers & distributors, New Delhi, 2004.

  10. 10. Ewing, GW. Instrumental methods of chemical analysis, 5th ed., McGraw Hill Book Company, New York, 1985.

  11. 11. Schirmer, RE. Modem methods of pharmaceutical analysis, Vol. I & II, 2nd ed., CRC Press, Florida, 2000.


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